C₄₅H₈₂O₈Si₃

Base Information

Chemical Name:C₄₅H₈₂O₈Si₃
CAS No.:1325710-85-7
Molecular Formula:C₄₅H₈₂O₈Si₃
Molecular Weight:835.398
Hs Code.:

C<sub>45</sub>H<sub>82</sub>O<sub>8</sub>Si<sub>3</sub>

Synonyms:C₄₅H₈₂O₈Si₃

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Chemical Property of C₄₅H₈₂O₈Si₃

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Technology Process of C₄₅H₈₂O₈Si₃

There total 12 articles about C₄₅H₈₂O₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1325710-84-6
C₁₈H₂₄O₄

: 1325710-61-9
C₂₉H₆₂O₄Si₃

: 1325710-85-7
C₄₅H₈₂O₈Si₃

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol201920j

Reference yield:

: 913066-81-6
[(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

: 1325710-85-7
C₄₅H₈₂O₈Si₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water / 2 h / pH 7 / Inert atmosphere; aq. buffer

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 1 h / 0 °C / Inert atmosphere

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 18 h / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; sodium periodate; osmium(VIII) oxide; potassium tert-butylate; sodium hydride; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; mineral oil; 3.1: Wittig reaction / 3.2: Wittig reaction;
DOI:10.1021/ol201920j

Reference yield:

: C₁₇H₂₂O₅

: 1325710-85-7
C₄₅H₈₂O₈Si₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 18 h / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; potassium tert-butylate; In tetrahydrofuran; toluene; 1.1: Wittig reaction / 1.2: Wittig reaction;
DOI:10.1021/ol201920j