N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline

Base Information

• Chemical Name: N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline
• CAS No.: 891861-84-0
• Molecular Formula: C₁₀H₁₁N₃O₄
• Molecular Weight: 237.215
• Mol file: 891861-84-0.mol

Synonyms:N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline

Chemical Property of N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline

There total 3 articles about N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-methyl-2,4-dinitroaniline (2044-88-4) + allyl bromide (106-95-6) → N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline (891861-84-0)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 70 ℃; for 14h;

DOI:10.1039/b601151a

Reference yield: 55.0%

N,N-dimethyl-2-propen-1-amine (2155-94-4) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → N,N-dimethyl-2,4-dinitroaniline (1670-17-3) + N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline (891861-84-0)

Guidance literature:

With tris[2-phenylpyridinato-C₂,N]iridium(III); N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 20 ℃; for 30h; Irradiation;

DOI:10.3390/molecules26113323

Reference yield:

N-methyl-N-allylamine (627-37-2) + 1-chloro-2,4-dinitro-benzene (97-00-7) → N-methyl-2,4-dinitro-N-prop-2-en-1-ylaniline (891861-84-0)

Guidance literature:

With ethanol; potassium acetate;

DOI:10.1021/ja01239a040

upstream raw materials:

N-methyl-N-allylamine

1-chloro-2,4-dinitro-benzene

N-methyl-2,4-dinitroaniline

allyl bromide