4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride

Base Information

Chemical Name:4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride
CAS No.:1179329-74-8
Molecular Formula:C₂₇H₂₁ClF₃N₅O₅S
Molecular Weight:620.008
Hs Code.:

Synonyms:4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride

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Chemical Property of 4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride

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Technology Process of 4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride

There total 7 articles about 4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1006898-92-5
4-[3-(2-aminobenzyl)-4,4-dimethyl-2,5-dioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

: 6752-38-1
4-chlorosulfonylbenzene isocyanate

: 1179329-74-8
4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride

Guidance literature:: In tetrahydrofuran; at 20 ℃;

Reference yield:

: 143782-20-1
4-(4,4-dimethyl-2,5-dioxoimidazolidin-1-yl)-2-(trifluoromethyl)benzonitrile

: 1179329-74-8
4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 5 h / 20 °C

2.1: caesium carbonate; Benzophenone imine / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 6 h / 95 °C / Inert atmosphere

2.2: 0.17 h / 20 °C

3.1: tetrahydrofuran / 20 °C

With Benzophenone imine; potassium carbonate; caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; acetonitrile;

Reference yield:

: 654-70-6
4-amino-2-trifluoromethylbenzonitrile

: 1179329-74-8
4-(3-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxoimidazolidin-1-ylmethyl]phenyl}ureido)benzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene; acetonitrile / 70 °C

1.2: 20 °C

1.3: 1 h / 70 °C

2.1: potassium carbonate / acetonitrile / 5 h / 20 °C

3.1: caesium carbonate; Benzophenone imine / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 6 h / 95 °C / Inert atmosphere

3.2: 0.17 h / 20 °C

4.1: tetrahydrofuran / 20 °C

With Benzophenone imine; potassium carbonate; caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; toluene; acetonitrile;