thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate

Base Information

Chemical Name:thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate
CAS No.:1428536-19-9
Molecular Formula:C₂HF₃O₂*C₁₅H₂₂N₂O₂S
Molecular Weight:408.442
Hs Code.:

Synonyms:thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate

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Chemical Property of thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate

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Technology Process of thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate

There total 9 articles about thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1428536-17-7
thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

: 76-05-1
trifluoroacetic acid

: 1428536-19-9
thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 5h; Temperature; Time;

Reference yield:

: 62-53-3
aniline

: 1428536-19-9
thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 20 °C

1.2: 2 h / 20 °C

2.1: 2,2'-azobis(isobutyronitrile) / 1,4-dioxane / 1 h / 75 °C

3.1: dichloromethane / 5 h / 20 °C

With 2,2'-azobis(isobutyronitrile); N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane;

Reference yield:

: ((S)-1-phenylcarbamoyl-hex-5-enyl)-carbamic acid tert-butyl ester

: 1428536-19-9
thioacetic acid S-((-S)-6-amino-6-phenylcarbamoyl-hexyl) ester trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-azobis(isobutyronitrile) / 1,4-dioxane / 1 h / 75 °C

2: dichloromethane / 5 h / 20 °C

With 2,2'-azobis(isobutyronitrile); In 1,4-dioxane; dichloromethane;