thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

Base Information

Chemical Name:thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester
CAS No.:1428536-17-7
Molecular Formula:C₂₀H₃₀N₂O₄S
Molecular Weight:394.535
Hs Code.:

Synonyms:thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

Suppliers and Price of thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

There total 9 articles about thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 908859-97-2
((S)-6-bromo-1-phenylcarbamoyl-hexyl)-carbamic acid tert-butyl ester

: 10387-40-3
potassium thioacetate

: 1428536-17-7
thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

Guidance literature:: In ethanol; at 20 ℃;

Reference yield:

: 62-53-3
aniline

: 1428536-17-7
thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 20 °C

1.2: 2 h / 20 °C

2.1: 2,2'-azobis(isobutyronitrile) / 1,4-dioxane / 1 h / 75 °C

With 2,2'-azobis(isobutyronitrile); N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane;

Reference yield:

: 204711-97-7
(2S)-2-[(tert-butoxycarbonyl)amino]hept-6-enoic acid

: 1428536-17-7
thioacetic acid S-((S)-6-tert-butoxycarbonylamino-6-phenylcarbamoyl-hexyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 20 °C

1.2: 2 h / 20 °C

2.1: 2,2'-azobis(isobutyronitrile) / 1,4-dioxane / 1 h / 75 °C

With 2,2'-azobis(isobutyronitrile); N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane;