3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate

Base Information

Chemical Name:3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate
CAS No.:1451274-40-0
Molecular Formula:C₁₇H₁₂BrF₃N₂O₆S₂
Molecular Weight:541.323
Hs Code.:

Synonyms:3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate

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Chemical Property of 3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate

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Technology Process of 3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate

There total 7 articles about 3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 1451273-43-0
5-bromo-N-(6-hydroxyquinolin-3-yl)-2-methoxybenzenesulfonamide

: 1451274-40-0
3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 1451274-40-0
3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: chlorosulfonic acid / 16 h / 25 °C

2: pyridine / 12 h / 40 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With pyridine; chlorosulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

Reference yield:

: 23095-05-8
5-bromo-2-methoxybenzenesulfonyl chloride

: 1451274-40-0
3-(5-bromo-2-methoxyphenylsulfonamido)quinolin-6-yltrifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 12 h / 40 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With pyridine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;