<2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate

Base Information

Chemical Name:<2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate
CAS No.:133415-58-4
Molecular Formula:C₁₉H₂₀O₆
Molecular Weight:344.364
Hs Code.:

Synonyms:<2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate

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Chemical Property of <2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate

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Technology Process of <2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate

There total 2 articles about <2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1885-14-9
phenyl chloroformate

: 133415-58-4
<2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 2 h / Ambient temperature

2: camphorsulfonic acid (CSA) / toluene / 18 h / Ambient temperature

With pyridine; camphor-10-sulfonic acid; In dichloromethane; toluene;
DOI:10.1021/jm00105a058

Reference yield:

: 60656-87-3
benzyloxyacetoaldehyde

: 100899-56-7
2,2-Dimethyl-4-phenoxycarbonyloxymethyl-1,3-dioxolane

: 133415-58-4
<2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate

Guidance literature:: With camphor-10-sulfonic acid; In toluene; for 18h; Yield given; Ambient temperature;
DOI:10.1021/jm00105a058

Reference yield: 93.0%

: 133415-58-4
<2-<(benzyloxy)methyl>-1,3-dioxolan-4-yl>methyl phenylcarbonate

: 131729-76-5
Carbonic acid 2-hydroxymethyl-[1,3]dioxolan-4-ylmethyl ester phenyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; for 18h; under 4137.2 Torr;
DOI:10.1021/jm00105a058