1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

Base Information

Chemical Name:1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole
CAS No.:1426812-04-5
Molecular Formula:C₆₀H₃₇N₅
Molecular Weight:827.987
Hs Code.:

Synonyms:1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

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Chemical Property of 1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

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Technology Process of 1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

There total 6 articles about 1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1426812-05-6
9-(4-formylphenyl)-9H-carbazole-3-carbaldehyde

: 62-53-3
aniline

: 84-11-7
9,10-phenanthrenequinone

: 1426812-04-5
1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: With ammonium acetate; In acetic acid; at 120 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201203335

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 1426812-04-5
1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; 18-crown-6 ether; copper(l) iodide / 1,2-dichloro-benzene / 48 h / 180 °C / Inert atmosphere

2: trichlorophosphate / 0 °C / Inert atmosphere

3: ammonium acetate / acetic acid / 2 h / 120 °C / Inert atmosphere

With copper(l) iodide; 18-crown-6 ether; ammonium acetate; potassium carbonate; trichlorophosphate; In acetic acid; 1,2-dichloro-benzene;
DOI:10.1002/chem.201203335

Reference yield:

: 57102-42-8
N-(4-bromophenyl)carbazole

: 1426812-04-5
1-phenyl-2-(4-(3-(1-phenyl-1H-phenanthro[9,10-d]imidazol-2-yl)-9H-carbazol-9-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / 12 h / 20 °C / Inert atmosphere

2: n-butyllithium / tetrahydrofuran / 7 h / -78 °C / Inert atmosphere

3: ammonium acetate; acetic acid / 2 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; n-butyllithium; ammonium acetate; acetic acid; In tetrahydrofuran;
DOI:10.1016/j.orgel.2014.07.019