N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff

Base Information

Chemical Name:N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff
CAS No.:154474-76-7
Molecular Formula:C₂₇H₃₈N₄O₄S
Molecular Weight:514.689
Hs Code.:

Synonyms:N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff

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Chemical Property of N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff

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Technology Process of N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff

There total 4 articles about N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 108467-99-8
1-(N-Boc-aminomethyl)-3-(aminomethyl)benzene

: 154474-76-7
N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff

Guidance literature:: In dichloromethane; for 24h;

Reference yield:

: 1477-55-0
1,3-di(aminomethyl)benzene

: 154474-76-7
N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / 0.5M aq. NaOH / dioxane / 15 h / Ambient temperature

2: 63 percent / HCl / diethyl ether / 0.5 h

3: 70 percent / CH₂Cl₂ / 24 h

With hydrogenchloride; sodium hydroxide; In 1,4-dioxane; diethyl ether; dichloromethane;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 154474-76-7
N,N'-Bis<3-(tert-butyloxycarbonylaminomethyl)phenylmethyl>thioharnstoff

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / 0.5M aq. NaOH / dioxane / 15 h / Ambient temperature

2: 63 percent / HCl / diethyl ether / 0.5 h

3: 70 percent / CH₂Cl₂ / 24 h

With hydrogenchloride; sodium hydroxide; In 1,4-dioxane; diethyl ether; dichloromethane;