(4-carboxyanilino)phenyl phenylsulfone

Base Information

Chemical Name:(4-carboxyanilino)phenyl phenylsulfone
CAS No.:114194-15-9
Molecular Formula:C₁₉H₁₅NO₃S
Molecular Weight:337.399
Hs Code.:

Synonyms:(4-carboxyanilino)phenyl phenylsulfone

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Chemical Property of (4-carboxyanilino)phenyl phenylsulfone

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Technology Process of (4-carboxyanilino)phenyl phenylsulfone

There total 2 articles about (4-carboxyanilino)phenyl phenylsulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 80-00-2,8012-45-1
4-Chlorophenyl phenyl sulfone

: 201230-82-2
carbon monoxide

: 62-53-3
aniline

: 114194-15-9
(4-carboxyanilino)phenyl phenylsulfone

Guidance literature:: With bis(triphenylphosphine)palladium(II)-chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,2-bis-(diphenylphosphino)ethane; sodium iodide; In N,N-dimethyl acetamide; at 115 ℃; for 6h; various conditions: CO pressure (5-95 psig) and periods of time (4-32 h); further reagents: tri-o-tolylphosphine, tri-p-tolylphosphine, Ph₃P;
DOI:10.1021/jo960861j

Reference yield:

: 37991-83-6
4-(phenylsulfonyl)benzoyl chloride

: 62-53-3
aniline

: 114194-15-9
(4-carboxyanilino)phenyl phenylsulfone

Guidance literature:: With benzene;

Reference yield:

: 114194-15-9
(4-carboxyanilino)phenyl phenylsulfone

: 66-39-7
4-(phenylsulfonyl)benzaldehyde

Guidance literature:: With phosphorus pentachloride; 1,1,2,2-tetrachloroethane; at 140 ℃; Schuetteln einer Loesung des erhaltenen Chlorimins in Tetrachloraethan mit SnCl₂ in aether.HCl und Erwaermen des Reaktionsprodukts mit wss.HCl;
DOI:10.1039/jr9480000601