Technology Process of C28H26O8S2
There total 5 articles about C28H26O8S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium fluoride; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride;
In
methanol; toluene;
at 55 ℃;
for 1.5h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-Bromosuccinimide; acetic acid / chloroform / 72 h / 0 - 20 °C
2: potassium fluoride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; bis(pinacol)diborane / toluene; methanol / 0.5 h / 80 °C / Inert atmosphere; Sealed tube
3: N-Bromosuccinimide; acetic acid / chloroform / 20 °C
4: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium fluoride / toluene; methanol / 1.5 h / 55 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; N-Bromosuccinimide; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; acetic acid; bis(pinacol)diborane;
In
methanol; chloroform; toluene;
4: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: acetyl chloride / 0 - 20 °C
2: N-Bromosuccinimide; acetic acid / chloroform / 72 h / 0 - 20 °C
3: potassium fluoride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; bis(pinacol)diborane / toluene; methanol / 0.5 h / 80 °C / Inert atmosphere; Sealed tube
4: N-Bromosuccinimide; acetic acid / chloroform / 20 °C
5: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium fluoride / toluene; methanol / 1.5 h / 55 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; N-Bromosuccinimide; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; acetic acid; acetyl chloride; bis(pinacol)diborane;
In
methanol; chloroform; toluene;
5: |Suzuki Coupling;