3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine

Base Information

Chemical Name:3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine
CAS No.:320410-12-6
Molecular Formula:C₂₃H₃₆BNO₄
Molecular Weight:401.354
Hs Code.:

Synonyms:3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine

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Chemical Property of 3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine

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Technology Process of 3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine

There total 1 articles about 3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 281681-21-8
3-[(4S,5S)-4,5-Bis(1-methoxycyclopentyl)-1,3,2-dioxoborolan-2-yl]propiophenone O-methyloxime

: 320410-12-6
3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1039/b005837h

Reference yield:

: 320410-12-6
3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine

: 82769-76-4
(S)-3-amino-3-phenylpropanol

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; for 1h; Heating;
DOI:10.1039/b005837h

Reference yield:

: 320410-12-6
3-[(4S,5S)-4,5-Bis-(1-methoxy-cyclopentyl)-[1,3,2]dioxaborolan-2-yl]-1-phenyl-propylamine

: (S)-1-acetoxy-3-acetylamino-3-phenylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH; H₂O₂ / 1 h / Heating

2: 96 percent / pyridine / tetrahydrofuran / 2 h / 20 °C

With pyridine; sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; 1: Hydrolysis / 2: Acetylation;
DOI:10.1039/b005837h