methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide

Base Information

Chemical Name:methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide
CAS No.:265994-15-8
Molecular Formula:C₁₇H₁₇BrFNO₄S
Molecular Weight:430.295
Hs Code.:

Synonyms:methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide

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Technology Process of methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide

There total 1 articles about methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29431-37-6
tetrahydrothiopyran-3-one-1,1-dioxide

: 14205-39-1
methyl (E)-3-aminocrotonate

: 77771-02-9
3-bromo-4-fluorobenzaldehyde

: 265994-15-8
methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide

Guidance literature:: In methanol; at 65 ℃; for 24h;
DOI:10.1021/jm030357o

Reference yield:

: 265994-15-8
methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide

: 265993-36-0
9-(3-bromo-4-fluoro-phenyl)-8,8-dioxo-4,5,6,7,8,9-hexahydro-3H-2-oxa-8λ⁶-thia-4-aza-cyclopenta[b]naphthalen-1-one

Guidance literature:: methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide; With pyridine; pyridinium hydrobromide perbromide; In chloroform; at -10 ℃; for 1h;

at 130 ℃; for 0.25h;
DOI:10.1021/jm030357o

Reference yield:

: 74-89-5
methylamine

: 265994-15-8
methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide

: 9-(3-bromo-4-fluoro-phenyl)-2-methyl-8,8-dioxo-2,3,4,5,6,7,8,9-octahydro-8λ⁶-thia-2,4-diaza-cyclopenta[b]naphthalen-1-one

Guidance literature:: methyl 8-(3-bromo-4-fluorophenyl)-6-methyl-3,4,5,8-tetrahydro-2H-thiopyrano[3,2-b]pyridine-7-carboxylate 1,1-dioxide; With pyridine; pyridinium hydrobromide perbromide; In chloroform; at -10 ℃; for 1h;

methylamine; In methanol; at 20 ℃; for 16h;
DOI:10.1021/jm030357o