5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide

Base Information

Chemical Name:5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide
CAS No.:916889-50-4
Molecular Formula:C₁₄H₁₆BrN₅O₂S
Molecular Weight:398.283
Hs Code.:

Synonyms:5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide

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Chemical Property of 5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide

Chemical Property:

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Technology Process of 5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide

There total 6 articles about 5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 916889-38-8
5-[4-(2-bromophenoxy)piperidin-1-yl]-1,3,4-thiadiazole-2-carbonitrile

: 916889-50-4
5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide

Guidance literature:: With hydroxylamine hydrochloride; potassium carbonate; In ethanol; at 20 ℃;

Reference yield:

: 109384-19-2
t-butyl 4-hydroxy piperidine-1-carboxylate

: 916889-50-4
5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 3 h / 0 °C

2: caesium carbonate / N,N-dimethyl-formamide / 70 °C

3: hydrogenchloride / ethanol / 12 h / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 4 h / 90 °C

5: hydroxylamine hydrochloride; potassium carbonate / ethanol / 20 °C

With hydrogenchloride; hydroxylamine hydrochloride; potassium carbonate; caesium carbonate; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 916889-48-0
4-(2-bromophenoxy)-piperidine hydrochloride

: 916889-50-4
5-[4-(2-bromophenoxy)piperidin-1-yl]-N'-hydroxy-1,3,4-thiadiazole-2-carboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 90 °C

2: hydroxylamine hydrochloride; potassium carbonate / ethanol / 20 °C

With hydroxylamine hydrochloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;