1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane

Base Information

Chemical Name:1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane
CAS No.:904325-43-5
Molecular Formula:C₃₀H₃₁N₂O₆P
Molecular Weight:546.56
Hs Code.:

Synonyms:1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane

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Chemical Property of 1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane

Chemical Property:

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Technology Process of 1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane

There total 6 articles about 1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 904325-42-4
1-{2-[N-benzyl-N-(tert-butyloxycarbonyl)amino]phenyl}-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane

: 904325-43-5
1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2006.03.063

Reference yield:

: 904325-40-2
2-{2-[N-benzyl-N-(tert-butyloxycarbonyl)amino]phenyl}ethanal

: 904325-43-5
1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / potassium tert-butoxide / acetonitrile; 2-methyl-propan-2-ol

2: 94 percent / DMAP / CH₂Cl₂ / 20 °C

3: 98 percent / trifluoroacetic acid / CH₂Cl₂ / 20 °C

With dmap; potassium tert-butylate; trifluoroacetic acid; In dichloromethane; acetonitrile; tert-butyl alcohol; 1: Henry reaction;
DOI:10.1016/j.tet.2006.03.063

Reference yield:

: 904325-39-9
2-{2-[N-benzyl-N-(tert-butyloxycarbonyl)amino]phenyl}ethanol

: 904325-43-5
1-[2-(N-benzylamino)phenyl]-3-methyl-3-nitro-2-(diphenylphosphatoxy)-butane

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / PCC; molecular sieves 4 Angstroem / CH₂Cl₂

2: 92 percent / potassium tert-butoxide / acetonitrile; 2-methyl-propan-2-ol

3: 94 percent / DMAP / CH₂Cl₂ / 20 °C

4: 98 percent / trifluoroacetic acid / CH₂Cl₂ / 20 °C

With dmap; 4 A molecular sieve; potassium tert-butylate; pyridinium chlorochromate; trifluoroacetic acid; In dichloromethane; acetonitrile; tert-butyl alcohol; 2: Henry reaction;
DOI:10.1016/j.tet.2006.03.063