S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate

Base Information

Chemical Name:S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate
CAS No.:1454839-24-7
Molecular Formula:C₂₃H₂₉NO₁₂S
Molecular Weight:543.549
Hs Code.:

Synonyms:S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate

Suppliers and Price of S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate

There total 3 articles about S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 19879-84-6
tetraacetyl thioglucose

: 105363-12-0
N-hydroxy-3,4-dimethoxybenzenecarboximidoyl chloride

: 1454839-24-7
S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane; at 20 ℃; for 2h; stereospecific reaction; Inert atmosphere;
DOI:10.1016/j.bmc.2013.07.049

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 1454839-24-7
S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride; pyridine / methanol / 2.5 h / 20 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 35 °C / Cooling with ice

3: triethylamine / dichloromethane; diethyl ether / 2 h / 20 °C / Inert atmosphere

With pyridine; N-chloro-succinimide; hydroxylamine hydrochloride; triethylamine; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.07.049

Reference yield:

: 2169-98-4,39627-82-2
3,4-Dimethoxy-benzaldehyde oxime

: 1454839-24-7
S-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-3,4-dimethoxyphenylthiohydroxamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide / N,N-dimethyl-formamide / 35 °C / Cooling with ice

2: triethylamine / dichloromethane; diethyl ether / 2 h / 20 °C / Inert atmosphere

With N-chloro-succinimide; triethylamine; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2013.07.049