N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl)-2-thioxoacetamide

Base Information

Chemical Name:N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl)-2-thioxoacetamide
CAS No.:1293389-48-6
Molecular Formula:C₁₄H₁₃N₅OS₂
Molecular Weight:331.422
Hs Code.:

Synonyms:N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl)-2-thioxoacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl)-2-thioxoacetamide

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Technology Process of N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl)-2-thioxoacetamide

There total 1 articles about N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl)-2-thioxoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 36273-89-9
4-(2-pyridyl)-3-thiosemicarbazide

: 532-55-8
Benzoyl isothiocyanate

: 1293389-48-6
N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl)-2-thioxoacetamide

Guidance literature:: In ethanol; Heating;
DOI:10.1016/j.molstruc.2011.08.020

Reference yield: 88.0%

: cobalt(II) chloride hexahydrate

: 1293389-48-6
N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl)-2-thioxoacetamide

: [Co(N-phenyl-2-(2-(pyridin-2-ylcarbamothioyl)hydrazinyl-2-thioxoacetamide)(H₂O)]*2H₂O

Guidance literature:: In ethanol; soln. was refluxed for 2-3 h; ppt. was filtered off, washed with EtOH and Et2O, dried in vac. over CaCl2; elem. anal.;
DOI:10.1016/j.molstruc.2011.08.020