methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside

Base Information

Chemical Name:methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside
CAS No.:1314132-21-2
Molecular Formula:C₅₀H₄₉NO₇
Molecular Weight:775.942
Hs Code.:

Synonyms:methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside

Suppliers and Price of methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside

There total 7 articles about methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-56-1
methanol

: C₄₉H₄₇NO₇

: 1314132-21-2
methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1002/chem.201003721

Reference yield:

: 1314132-47-2
(2R,3R,4S,5R)-5-(N-fluorenylmethoxycarbonyl)benzylamino-2,3,4-tribenzyloxyhept-6-en-1-ol

: 1314132-21-2
methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: ozone / dichloromethane / 0.58 h / -78 °C

1.2: 24 h / -78 °C

2.1: toluene-4-sulfonic acid / dichloromethane / 8 h / 20 °C / Inert atmosphere

With toluene-4-sulfonic acid; ozone; In dichloromethane;
DOI:10.1002/chem.201003721

Reference yield:

: 1314279-65-6
(2R,3R,4S,5R)-5-(N-benzylamino)-2,3,4-tris-(benzyloxy)-hept-6-en-1-ol

: 1314132-21-2
methyl α-2-(N-benzyl-N-fluorenylmethoxycarbonylamino)-3,4,5-tri-O-benzyl-2-deoxy-D-idoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 3 h / Inert atmosphere

2.1: ozone / dichloromethane / 0.58 h / -78 °C

2.2: 24 h / -78 °C

3.1: toluene-4-sulfonic acid / dichloromethane / 8 h / 20 °C / Inert atmosphere

With toluene-4-sulfonic acid; ozone; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1002/chem.201003721