N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide

Base Information

Chemical Name:N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide
CAS No.:1245034-88-1
Molecular Formula:C₂₈H₃₃N₃O₃S
Molecular Weight:491.654
Hs Code.:

Synonyms:N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide

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Chemical Property of N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide

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Technology Process of N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide

There total 6 articles about N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 377769-51-2
5-(N-(4-butylphenyl)sulfamoyl)-2-methylbenzoic acid

: 4004-95-9,70849-66-0,2210-93-7
1-phenylpiperazine hydrochloride

: 1245034-88-1
N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide

Guidance literature:: 1-phenylpiperazine hydrochloride; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

5-(N-(4-butylphenyl)sulfamoyl)-2-methylbenzoic acid; With benzotriazol-1-ol; In N,N-dimethyl-formamide; at 0 - 20 ℃;

Reference yield:

: 92-54-6
4-phenyl-1-piperazine

: 377769-51-2
5-(N-(4-butylphenyl)sulfamoyl)-2-methylbenzoic acid

: 1245034-88-1
N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide

Guidance literature:: 5-(N-(4-butylphenyl)sulfamoyl)-2-methylbenzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

4-phenyl-1-piperazine; In N,N-dimethyl-formamide; at 0 - 20 ℃;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1245034-88-1
N-(4-butylphenyl)-4-methyl-3-(4-phenylpiperazine-1-carbonyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 12 h / 90 °C / Inert atmosphere

2.1: hydrogenchloride / methanol / 2 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.08 h / 0 °C

3.2: 0 - 20 °C

With hydrogenchloride; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;