5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester

Base Information

• Chemical Name: 5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester
• CAS No.: 85590-40-5
• Molecular Formula: C₂₉H₂₆N₂O₅
• Molecular Weight: 482.536

Synonyms:5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester

Chemical Property of 5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester

Chemical Property:

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Technology Process of 5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester

There total 3 articles about 5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(E)-2-[1-(4-Methoxy-benzoyl)-2,2-bis-p-tolylamino-vinyl]-but-2-enedioic acid dimethyl ester (85590-31-4) → 5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester (85590-40-5)

Guidance literature:

With triethylamine; In methanol; at 80 - 90 ℃; for 6h;

DOI:10.1055/s-1983-30260

Reference yield:

1-(4-Methoxy-phenyl)-3,3-bis-p-tolylamino-propenone (85590-25-6) → 5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester (85590-40-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / benzene / 8 h / Ambient temperature

2: 65 percent / triethylamine / methanol / 6 h / 80 - 90 °C

With triethylamine; In methanol; benzene;

DOI:10.1055/s-1983-30260

Reference yield:

dimethyl acetylenedicarboxylate (762-42-5) → 5-(4-Methoxy-benzoyl)-2-oxo-1-p-tolyl-6-p-tolylamino-1,2-dihydro-pyridine-4-carboxylic acid methyl ester (85590-40-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / benzene / 8 h / Ambient temperature

2: 65 percent / triethylamine / methanol / 6 h / 80 - 90 °C

With triethylamine; In methanol; benzene;

DOI:10.1055/s-1983-30260

upstream raw materials:

(E)-2-[1-(4-Methoxy-benzoyl)-2,2-bis-p-tolylamino-vinyl]-but-2-enedioic acid dimethyl ester

1-(4-Methoxy-phenyl)-3,3-bis-p-tolylamino-propenone

dimethyl acetylenedicarboxylate

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