<methyl>dimethylphenylsilane

Base Information

Chemical Name:<methyl>dimethylphenylsilane
CAS No.:120743-93-3
Molecular Formula:C₂₁H₃₂OSi₂
Molecular Weight:356.655
Hs Code.:

<<o-(tert-butyldimethylsiloxy)phenyl>methyl>dimethylphenylsilane

Synonyms:<methyl>dimethylphenylsilane

Suppliers and Price of <methyl>dimethylphenylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <methyl>dimethylphenylsilane

Chemical Property:

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Technology Process of <methyl>dimethylphenylsilane

There total 2 articles about <methyl>dimethylphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62790-79-8
2-(tert-butyldimethylsilyloxy)toluene

: 120743-93-3
<methyl>dimethylphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: NBS, azobis(isobutyronitrile) / CCl₄ / 0.17 h / Heating

2: 1.) magnesium, ethylene dibromide / 1.) Et₂O, reflux, 15 min, 2.) 3 h

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); magnesium; ethylene dibromide; In tetrachloromethane;
DOI:10.1021/jo00273a033

Reference yield:

: 105262-86-0
2-((tert-butyldimethylsilyl)oxy)benzyl bromide

: 768-33-2
phenyldimethylsilyl chloride

: 120743-93-3
<methyl>dimethylphenylsilane

: C₂₆H₄₂O₂Si₂

Guidance literature:: With magnesium; ethylene dibromide; Yield given. Multistep reaction; 1.) Et₂O, reflux, 15 min, 2.) 3 h;
DOI:10.1021/jo00273a033