(L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate

Base Information

• Chemical Name: (L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate
• CAS No.: 1429195-00-5
• Molecular Formula: C₁₉H₂₄N₂O₅S
• Molecular Weight: 392.476

Synonyms:(L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate

Chemical Property of (L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate

Chemical Property:

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Technology Process of (L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate

There total 5 articles about (L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-methoxy-benzylamine (2393-23-9) + methyl (2S)-1-[(4-methylphenyl)sulfonyl]aziridine-2-carboxylate (105424-75-7) → (L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate (1429195-00-5) + (R)-methyl 2-(4-methoxybenzylamino)-3-(4-methylphenylsulfonamido)propanoate (1429195-01-6)

Guidance literature:

In acetonitrile; at 20 ℃; for 24h;

DOI:10.1016/j.tetlet.2013.02.096

Reference yield: 70.0%

4-methoxy-benzylamine (2393-23-9) + methyl (2S)-1-[(4-methylphenyl)sulfonyl]aziridine-2-carboxylate (105424-75-7) → (L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate (1429195-00-5) + (D)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate

Guidance literature:

In acetonitrile; at 20 ℃; for 24h; Temperature; regioselective reaction;

DOI:10.1016/j.tetlet.2013.09.116

Reference yield: 70.0%

4-methoxy-benzylamine (2393-23-9) + methyl (2S)-1-[(4-methylphenyl)sulfonyl]aziridine-2-carboxylate (105424-75-7) → (L)-methyl 3-(4-methoxybenzylamino)-2-(4-methylphenylsulfonamido)propanoate (1429195-00-5) + (R)-methyl 2-(4-methoxybenzylamino)-3-(4-methoxyphenylsulfonamido)propanoate

Guidance literature:

In acetonitrile; at 20 ℃; for 24h; regioselective reaction;

DOI:10.1016/j.tet.2014.06.011

upstream raw materials:

4-methoxy-benzylamine

methyl (2S)-1-[(4-methylphenyl)sulfonyl]aziridine-2-carboxylate

p-toluenesulfonyl chloride

Downstream raw materials:

(S)-methyl 3-(((S)-3-methoxy-2-(4-methylphenylsulfonamido)-3-oxopropyl)(4-methoxybenzyl)amino)-2-(4-nitrophenylsulfonamido)propanoate

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