(+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone

Base Information

Chemical Name:(+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone
CAS No.:1019857-17-0
Molecular Formula:C₂₅H₄₂O₄Si₂
Molecular Weight:462.777
Hs Code.:

Synonyms:(+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone

Suppliers and Price of (+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone

There total 1 articles about (+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1019857-16-9
(+/-)-5-[[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]hydroxymethyl]-2-cyclopentenone

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1019857-17-0
(+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/jo702635t

Reference yield: 59.0%

: 1019857-17-0
(+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone

: 1826-67-1
vinyl magnesium bromide

: (2RS,4RS)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-4-ethenylcyclopentanone

: (2RS,4SR)-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-4-ethenylcyclopentanone

Guidance literature:: vinyl magnesium bromide; With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -78 ℃; for 0.333333h;

(+/-)-5-[[[(1,1-dimethylethyl)dimethylsilyl]oxy][3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-methoxyphenyl]methyl]-2-cyclopentenone; In tetrahydrofuran; at -78 - 0 ℃; for 3h; Further stages.;
DOI:10.1021/jo702635t