2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether

Base Information

Chemical Name:2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether
CAS No.:116740-30-8
Molecular Formula:C₁₇H₂₃F₃O₄S
Molecular Weight:380.428
Hs Code.:

Synonyms:2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether

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Chemical Property of 2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether

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Technology Process of 2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether

There total 4 articles about 2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 2-methyl-4-phenylsulfonyl-3-trifluoromethyl-2-butanol

: 116740-30-8
2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether

Guidance literature:: With sodium hydroxide; In 1,4-dioxane;

Reference yield:

: 102687-63-8
(E)-((3,3,3-trifluoroprop-1-en-1-yl)sulfonyl)benzene

: 116740-30-8
2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / LDA, / tetrahydrofuran

2: 1,) DIBAL, 2,) 10percent HCl / 1.)Et₂O 2.) MeOH

With hydrogenchloride; diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)80061-1

Reference yield:

: 116355-89-6
2-methyl-4-phenylsulfonyl-2-triethylsiloxy-3-trifluoromethylbutyric acid ethyl ester

: 116740-30-8
2-methyl-4 phenylsulfonyl-3-trifluoromethyl-2-butanol tetrahydropyranyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1,) DIBAL, 2,) 10percent HCl / 1.)Et₂O 2.) MeOH

With hydrogenchloride; diisobutylaluminium hydride;
DOI:10.1016/S0040-4039(00)80061-1