Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester

Base Information

Chemical Name:Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester
CAS No.:173677-11-7
Molecular Formula:C₃₂H₄₅NO₆
Molecular Weight:539.712
Hs Code.:

Synonyms:Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester

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Chemical Property of Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester

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Technology Process of Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester

There total 3 articles about Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 814-68-6,25189-84-8
acryloyl chloride

9-[(R)-1-(3,4-Dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonan-1-ol: 173677-08-2
9-[(R)-1-(3,4-Dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonan-1-ol

: 173677-11-7
Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester

Guidance literature:: With 2-hydroxyresorcinol; In benzene; at 40 ℃; for 1h;
DOI:10.1021/jm950477z

Reference yield:

: 55362-80-6
9-bromononan-1-ol

: 173677-11-7
Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / acetonitrile / 70 h / Heating

2: 74 percent / pyrogallol / benzene / 1 h / 40 °C

With 2-hydroxyresorcinol; In acetonitrile; benzene;
DOI:10.1021/jm950477z

Reference yield:

: 50896-90-7
(-) N-norlaudanosine

: 173677-11-7
Acrylic acid 9-[(R)-1-(3,4-dimethoxy-benzyl)-6,7-dimethoxy-3,4-dihydro-1H-isoquinolin-2-yl]-nonyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / acetonitrile / 70 h / Heating

2: 74 percent / pyrogallol / benzene / 1 h / 40 °C

With 2-hydroxyresorcinol; In acetonitrile; benzene;
DOI:10.1021/jm950477z