1-hydroperoxy-1-phenylcycloheptane

Base Information

• Chemical Name: 1-hydroperoxy-1-phenylcycloheptane
• CAS No.: 37908-41-1
• Molecular Formula: C₁₃H₁₈O₂
• Molecular Weight: 206.285
• Mol file: 37908-41-1.mol

Synonyms:1-hydroperoxy-1-phenylcycloheptane

Chemical Property of 1-hydroperoxy-1-phenylcycloheptane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-hydroperoxy-1-phenylcycloheptane

There total 3 articles about 1-hydroperoxy-1-phenylcycloheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

1-phenylcycloheptanol (2082-21-5) → 1-hydroperoxy-1-phenylcycloheptane (37908-41-1)

Guidance literature:

With sulfuric acid; dihydrogen peroxide; In water; at 0 - 20 ℃; for 18h; Inert atmosphere;

DOI:10.1016/j.tetlet.2021.153144

Reference yield:

phenylcycloheptane (4401-18-7) → 1-hydroperoxy-1-phenylcycloheptane (37908-41-1)

Guidance literature:

With oxygen; copper(II) phthalocyanine;

Reference yield:

Cycloheptene (628-92-2,45509-99-7) → 1-hydroperoxy-1-phenylcycloheptane (37908-41-1)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄

2: O₂ / copper phthalocyanine

With sulfuric acid; oxygen; copper(II) phthalocyanine;

upstream raw materials:

phenylcycloheptane

Cycloheptene

1-phenylcycloheptanol

Downstream raw materials:

ω-chloroheptanoylbenzene

7-bromo-1-phenylheptan-1-one

7-iodo-1-phenylheptan-1-one

8-oxo-8-phenyloctanenitrile