3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate

Base Information

Chemical Name:3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate
CAS No.:627091-60-5
Molecular Formula:C₁₆H₂₄Cl₃NO₂Si
Molecular Weight:396.817
Hs Code.:

Synonyms:3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate

Chemical Property:

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Technology Process of 3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate

There total 4 articles about 3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 681275-04-7
1-(3'-t-butyldimethylsilyloxyphenyl)ethanol

: 545-06-2
trichloroacetonitrile

: 627091-60-5
3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate

Guidance literature:: With sodium hydride; In diethyl ether; at -10 - 20 ℃;
DOI:10.1071/CH03027

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 627091-60-5
3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / imidazole / dimethylformamide / 12 h / 20 °C

2: 93 percent / lithium aluminium hydride / diethyl ether / 1 h

3: 90 percent / sodium hydride / diethyl ether / -10 - 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; sodium hydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1071/CH03027

Reference yield:

: 124414-07-9
1-(3-{[tert-butyl(dimethyl)silyl]oxy}phenyl)ethanone

: 627091-60-5
3'-t-butyldimethylsilyloxy-α'-methylbenzyl 2,2,2-trichloroethanimidate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / lithium aluminium hydride / diethyl ether / 1 h

2: 90 percent / sodium hydride / diethyl ether / -10 - 20 °C

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether;
DOI:10.1071/CH03027