3,5-bis(tri?uoromethyl)phenyl phenyl sulfide

Base Information

Chemical Name:3,5-bis(tri?uoromethyl)phenyl phenyl sulfide
CAS No.:58324-87-1
Molecular Formula:C₁₄H₈F₆S
Molecular Weight:322.274
Hs Code.:

Synonyms:3,5-bis(tri?uoromethyl)phenyl phenyl sulfide

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Chemical Property of 3,5-bis(tri?uoromethyl)phenyl phenyl sulfide

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Technology Process of 3,5-bis(tri?uoromethyl)phenyl phenyl sulfide

There total 9 articles about 3,5-bis(tri?uoromethyl)phenyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 328-70-1
3,6-bis(trifluoromethyl)bromobenzene

: 108-98-5
thiophenol

: 58324-87-1
3,5-bis(tri?uoromethyl)phenyl phenyl sulfide

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; In toluene; for 3h; Inert atmosphere; Reflux;
DOI:10.1055/s-0030-1259012

Reference yield: 88.0%

: 402-31-3
1,3-bis(trifluoromethyl)benzene

: 882-33-7
diphenyldisulfane

: 58324-87-1
3,5-bis(tri?uoromethyl)phenyl phenyl sulfide

Guidance literature:: 1,3-bis(trifluoromethyl)benzene; With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; bis(pinacol)diborane; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; at 80 ℃; for 24h; Inert atmosphere;

diphenyldisulfane; With [2,2]bipyridinyl; copper(l) chloride; In water; dimethyl sulfoxide; at 80 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c2cc33950a

Reference yield: 72.0%

: 328-73-4
3,5-bis(trifluoromethyl)iodobenzene

: 108-98-5
thiophenol

: 58324-87-1
3,5-bis(tri?uoromethyl)phenyl phenyl sulfide

Guidance literature:: With copper(l) iodide; 3,5-dimethyl-1-((phenylselenyl)methyl)-1H-pyrazole; caesium carbonate; In dimethyl sulfoxide; at 110 ℃; for 6h;
DOI:10.1016/j.catcom.2018.12.009