1-Dodecylpiperidine

Base Information

• Chemical Name: 1-Dodecylpiperidine
• CAS No.: 5917-47-5
• Molecular Formula: C17H35 N
• Molecular Weight: 253.472
• European Community (EC) Number: 227-641-0
• DSSTox Substance ID: DTXSID9064059
• Nikkaji Number: J223.880B
• Wikidata: Q81991210
• Mol file: 5917-47-5.mol

Synonyms:1-Dodecylpiperidine;Piperidine, 1-dodecyl-;5917-47-5;N-Dodecylpiperidine;EINECS 227-641-0;AI3-08183;SCHEMBL1262658;DTXSID9064059;C17H35N;AKOS024341268

Chemical Property of 1-Dodecylpiperidine

Chemical Property:

• Vapor Pressure: 0.000314mmHg at 25°C
• Refractive Index: 1.4588 (estimate)
• Boiling Point: 320.6°Cat760mmHg
• Flash Point: 180.9°C
• PSA: 3.24000
• Density: 0.844g/cm³
• LogP: 5.33110
• XLogP3: 6.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 11
• Exact Mass: 253.276950121
• Heavy Atom Count: 18
• Complexity: 161

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCN1CCCCC1

Technology Process of 1-Dodecylpiperidine

There total 14 articles about 1-Dodecylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

piperidine (110-89-4) + 1-dodecylbromide (143-15-7) → 1-dodecylpiperidine (5917-47-5)

Guidance literature:

With potassium carbonate; In acetonitrile; Heating;

DOI:10.1002/chem.200500613

Reference yield: 76.0%

1 ,5-pentanediol (111-29-5) + n-Dodecylamine (124-22-1) → 1-dodecylpiperidine (5917-47-5)

Guidance literature:

With ruthenium trichloride; tributylphosphine; In 1,4-dioxane; at 180 ℃; for 5h;

DOI:10.1021/jo00209a004

Reference yield:

N-dodecanoylpiperidine (22342-28-5) → 1-dodecylpiperidine (5917-47-5)

Guidance literature:

With 1,4-dioxane; copper oxide-chromium oxide; at 250 ℃; under 147102 - 220652 Torr; Hydrogenation;

DOI:10.1021/ja01326a061

upstream raw materials:

piperidine

1-dodecyl alcohol

1-Iodododecane

1-dodecylbromide

Downstream raw materials:

1-dodecyl-1-methylpiperidinium bromide

1-dodecyl-1-methyl-piperidinium; iodide

Refernces

• 1、 Bhadani, Avinash,Tani, Misako,Endo, Takeshi,Sakai, Kenichi,Abe, Masahiko,Sakai, Hideki. "New ester based gemini surfactants: the effect of different cationic headgroups on micellization properties and viscosity of aqueous micellar solution". . p. 19474 - 19483. Retrieved 2015/07/27.
• 2、 Kiuchi,Nishizawa,Kawanishi,Kinoshita,Ohsima,Uchitani,Sekino,Ishida,Kondo,Tsuda. "Nematocidal activity of long alkyl chain amides, amines and their derivatives on dog roundworm larvae". . p. 3234 - 3244. Retrieved 2007/10/02.