N,N-diphenyl pyridin-3-amine

Base Information

• Chemical Name: N,N-diphenyl pyridin-3-amine
• CAS No.: 133568-48-6
• Molecular Formula: C₁₇H₁₄N₂
• Molecular Weight: 246.312
• Mol file: 133568-48-6.mol

Synonyms:N,N-diphenyl pyridin-3-amine

Chemical Property of N,N-diphenyl pyridin-3-amine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N,N-diphenyl pyridin-3-amine

There total 6 articles about N,N-diphenyl pyridin-3-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-Bromopyridine (626-55-1,163928-56-1) + diphenylamine (122-39-4) → N,N-diphenyl pyridin-3-amine (133568-48-6)

Guidance literature:

With palladium diacetate; sodium t-butanolate; ruphos; In neat (no solvent); at 110 ℃; for 12h; Green chemistry;

DOI:10.1002/ejoc.201402077

Reference yield: 97.0%

3-Chloropyridine (626-60-8) + diphenylamine (122-39-4) → N,N-diphenyl pyridin-3-amine (133568-48-6)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; C₃₃H₄₈N₇P; sodium t-butanolate; In toluene; at 80 ℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1002/ejoc.201403428

Reference yield: 54.0%

pyridin-3-ylamine (462-08-8) + bromobenzene (108-86-1,52753-63-6) → N,N-diphenyl pyridin-3-amine (133568-48-6)

Guidance literature:

With copper(l) iodide; 18-crown-6 ether; potassium carbonate; at 150 ℃; Inert atmosphere;

DOI:10.1007/s00775-014-1133-6

upstream raw materials:

3-Bromopyridine

diphenylamine

3-Chloropyridine

pyridin-3-ylamine