Technology Process of C17H15BrN2
There total 3 articles about C17H15BrN2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
N-(2,6-dimethylphenyl)-3-bromobenzamide;
With
phosphorus pentachloride; trichlorophosphate;
for 16h;
Reflux;
Inert atmosphere;
2,2-dimethoxyethylamine;
In
isopropyl alcohol;
for 16h;
Inert atmosphere;
With
hydrogenchloride;
In
water; isopropyl alcohol;
for 20h;
Reflux;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridine / 16 h / 20 °C / Inert atmosphere
2.1: phosphorus pentachloride; trichlorophosphate / 16 h / Reflux; Inert atmosphere
2.2: 16 h / Inert atmosphere
2.3: 20 h / Reflux; Inert atmosphere
With
pyridine; phosphorus pentachloride; trichlorophosphate;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridine / 16 h / 20 °C / Inert atmosphere
2.1: phosphorus pentachloride; trichlorophosphate / 16 h / Reflux; Inert atmosphere
2.2: 16 h / Inert atmosphere
2.3: 20 h / Reflux; Inert atmosphere
With
pyridine; phosphorus pentachloride; trichlorophosphate;