N-(tert-butoxycarbonyl)-3,4-(dimethoxy)-6-(iodo)-L-phenylalanine methyl ester

Base Information Edit

Chemical Name:N-(tert-butoxycarbonyl)-3,4-(dimethoxy)-6-(iodo)-L-phenylalanine methyl ester
CAS No.:1421282-27-0
Molecular Formula:C₁₇H₂₄INO₆
Molecular Weight:465.285
Hs Code.:
Mol file:1421282-27-0.mol

Synonyms:N-(tert-butoxycarbonyl)-3,4-(dimethoxy)-6-(iodo)-L-phenylalanine methyl ester

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Chemical Property of N-(tert-butoxycarbonyl)-3,4-(dimethoxy)-6-(iodo)-L-phenylalanine methyl ester Edit

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Technology Process of N-(tert-butoxycarbonyl)-3,4-(dimethoxy)-6-(iodo)-L-phenylalanine methyl ester

There total 7 articles about N-(tert-butoxycarbonyl)-3,4-(dimethoxy)-6-(iodo)-L-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32161-30-1
(S)-3,4-dimethoxyphenylalanine

: 1421282-27-0
N-(tert-butoxycarbonyl)-3,4-(dimethoxy)-6-(iodo)-L-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 10 h / 0 °C / Reflux

2: trifluoroacetic acid; N-iodo-succinimide / acetonitrile / 18.33 h / Darkness

3: triethylamine; dmap / acetonitrile / 20 °C

With dmap; N-iodo-succinimide; thionyl chloride; triethylamine; trifluoroacetic acid; In acetonitrile;

Reference yield:

: C₁₇H₂₂INO₆

: 1421282-27-0
N-(tert-butoxycarbonyl)-3,4-(dimethoxy)-6-(iodo)-L-phenylalanine methyl ester

Guidance literature:: With hydrogen; (+)-1,2-bis((2S,5S)-2,5-diethylphosphorano)benzene(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; In methanol; ethyl acetate; under 1551.49 Torr;