(S)-ethyl 2-(N-(tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

Base Information

Chemical Name:(S)-ethyl 2-(N-(tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate
CAS No.:128217-62-9
Molecular Formula:C₁₈H₂₇NO₆
Molecular Weight:353.415
Hs Code.:

Synonyms:(S)-ethyl 2-(N-(tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-ethyl 2-(N-(tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

Chemical Property:

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Technology Process of (S)-ethyl 2-(N-(tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

There total 12 articles about (S)-ethyl 2-(N-(tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1313214-06-0
N-(tert-butoxycarbonyl)-3,4-(dihydroxy)-L-phenylalanine ethyl ester

: 74-88-4
methyl iodide

: 128217-62-9
(S)-ethyl 2-(N-(tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c2cc38646a

Reference yield:

: 2-tert-Butoxycarbonylamino-3-(3,4-dihydroxy-phenyl)-propionic acid ethyl ester

: 128217-61-8,128217-62-9
2-tert-Butoxycarbonylamino-3-(3,4-dimethoxy-phenyl)-propionic acid ethyl ester

Guidance literature:: With potassium carbonate; sodium iodide; In ethanol; for 4h; Yield given; Heating;
DOI:10.1021/jo00301a008

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 128217-61-8,128217-62-9
2-tert-Butoxycarbonylamino-3-(3,4-dimethoxy-phenyl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / H₂O; tetrahydrofuran / overnight

2: K₂CO₃, NaI / ethanol / 4 h / Heating

With sodium hydrogencarbonate; potassium carbonate; sodium iodide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jo00301a008