Technology Process of C26H27N7O3
There total 10 articles about C26H27N7O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonia;
In
isopropyl alcohol;
at 80 ℃;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: triethylsilane / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2.2: 1.5 h / 0 - 20 °C / Inert atmosphere
3.1: ammonia / isopropyl alcohol / 80 °C / Sealed tube
With
triethylsilane; ammonia; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium azide / water; acetone / 16 h / 50 °C / Large scale
1.2: 1 h / Large scale
2.1: hydrogenchloride / ethanol / 5 h / 83 °C / Large scale
3.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / -25 °C / Inert atmosphere
3.2: 2.2 h / 25 °C / Inert atmosphere
4.1: lithium diisopropyl amide / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere
4.2: 1 h / -78 °C / Inert atmosphere
5.1: triethylsilane / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
5.2: 1.5 h / 0 - 20 °C / Inert atmosphere
6.1: ammonia / isopropyl alcohol / 80 °C / Sealed tube
With
hydrogenchloride; triethylsilane; sodium azide; ammonia; sodium hydride; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetone;