2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.^2,5>trideca-Δ^1,9,10,12-trien-3-one

Base Information

• Chemical Name: 2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.^2,5>trideca-Δ^1,9,10,12-trien-3-one
• CAS No.: 116897-56-4
• Molecular Formula: C₂₉H₂₃NO₂S
• Molecular Weight: 449.573

Synonyms:2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.^2,5>trideca-Δ^1,9,10,12-trien-3-one

Chemical Property of 2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.^2,5>trideca-Δ^1,9,10,12-trien-3-one

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Technology Process of 2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.^2,5>trideca-Δ^1,9,10,12-trien-3-one

There total 3 articles about 2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.^2,5>trideca-Δ^1,9,10,12-trien-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,3-dihydro-2,4-diphenyl-1,5-benzothiazepine (40358-31-4) + Phenoxyacetyl chloride (701-99-5) → 2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.2,5>trideca-Δ1,9,10,12-trien-3-one (116897-56-4,936253-11-1)

Guidance literature:

With triethylamine; In benzene; at 20 ℃; for 4h;

DOI:10.1002/hc.10196

Reference yield: 52.0%

2-diazo-1-phenylethan-1-one (21119-50-6) + 2,3-dihydro-2,4-diphenyl-1,5-benzothiazepine (40358-31-4) → 2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.2,5>trideca-Δ1,9,10,12-trien-3-one (116897-56-4,936253-11-1)

Guidance literature:

In dichloromethane; at 20 ℃; for 6h; Inert atmosphere; UV-irradiation;

DOI:10.1055/s-0030-1259485

Reference yield:

2,3-dihydro-2,4-diphenyl-1,5-benzothiazepine (40358-31-4) + triethylamine (121-44-8) + Phenoxyacetyl chloride (701-99-5) → 2-aza-4-phenoxy-5,7-diphenyl-8-thiatricyclo<7.4.0.0.2,5>trideca-Δ1,9,10,12-trien-3-one (116897-56-4,936253-11-1)

Guidance literature:

Yield given. Multistep reaction; 1.) benzene, reflux; 2.) benzene, reflux, 60 min;

DOI:10.1139/v88-047

upstream raw materials:

2,3-dihydro-2,4-diphenyl-1,5-benzothiazepine

triethylamine

Phenoxyacetyl chloride

2-diazo-1-phenylethan-1-one

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