nickel(II) diphenylglyoxal-bis(S-methylisothiocarbohydrazonate)

Base Information Edit

Chemical Name:nickel(II) diphenylglyoxal-bis(S-methylisothiocarbohydrazonate)
CAS No.:150207-04-8
Molecular Formula:C₁₈H₂₀N₈NiS₂
Molecular Weight:471.232
Hs Code.:
Mol file:150207-04-8.mol

Synonyms:nickel(II) diphenylglyoxal-bis(S-methylisothiocarbohydrazonate)

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Chemical Property of nickel(II) diphenylglyoxal-bis(S-methylisothiocarbohydrazonate) Edit

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Technology Process of nickel(II) diphenylglyoxal-bis(S-methylisothiocarbohydrazonate)

There total 1 articles about nickel(II) diphenylglyoxal-bis(S-methylisothiocarbohydrazonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: nickel(II) chloride hexahydrate

: 37839-01-3,67708-03-6
1H(+)-S-methylisothiocarbonohydrazidium iodide

: 134-81-6
benzil

: 150207-04-8
nickel(II) diphenylglyoxal-bis(S-methylisothiocarbohydrazonate)

Guidance literature:: With NH₄OH; In ethanol; water; addn. of NiCl2 with 2.4 equiv. of carbohydrazide (in H2O) to diphenylglyoxal (in hot EtOH), addn. of 25% NH4OH, heating (water bath, 10 min, pptn.); hot filtration, washing (EtOH, CHCl3); elem. anal.;

Reference yield: 79.0%

: 150207-04-8
nickel(II) diphenylglyoxal-bis(S-methylisothiocarbohydrazonate)

: 134-81-6
benzil

: 105131-04-2
Ni(C₃₂H₂₆N₈S₂)

Guidance literature:: In N,N-dimethyl-formamide; 1.2 fold excesss of diphenyl glyoxal, heating (140-150°C, 4 h); filtration, washing (DMF, acetone);