5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle

Base Information

Chemical Name:5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle
CAS No.:143604-43-7
Molecular Formula:C₁₆H₂₅NO₆S
Molecular Weight:359.444
Hs Code.:

Synonyms:5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle

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Technology Process of 5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle

There total 7 articles about 5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124-63-0
methanesulfonyl chloride

: 143604-36-8
5-O-Benzyl-3-desoxy-3-dimethylamino-β-D-xylofuranoside de methyle

: 143604-43-7
5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle

Guidance literature:: With triethylamine; In dichloromethane; at -30 ℃; for 2.5h;
DOI:10.1016/S0040-4020(01)90122-X

Reference yield:

: 20535-09-5
2,3-Anhydro-5-O-benzyl-β-D-ribofuranoside de methyle

: 143604-43-7
5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle

Guidance literature:: Multi-step reaction with 5 steps

1: 22 percent / H₂O / 96 h / 100 °C

2: 97 percent / Et₃N / CH₂Cl₂ / 1.5 h / -30 °C

3: CD₃CN, D₂O / 2 h / 75 °C

4: H₂O / 20 h / 70 °C

5: 100 percent / Et₃N / CH₂Cl₂ / 2.5 h / -30 °C

With [D₃]acetonitrile; water; water-d2; triethylamine; In dichloromethane; water;
DOI:10.1016/S0040-4020(01)90122-X

Reference yield:

: 100-39-0
benzyl bromide

: 143604-43-7
5-O-Benzyl-3-desoxy-3-dimethylamino-2-O-methanesulfonyl-β-D-xylofuranoside de methyle

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / NaH / tetrahydrofuran / 2.5 h

2: 22 percent / H₂O / 96 h / 100 °C

3: 97 percent / Et₃N / CH₂Cl₂ / 1.5 h / -30 °C

4: CD₃CN, D₂O / 2 h / 75 °C

5: H₂O / 20 h / 70 °C

6: 100 percent / Et₃N / CH₂Cl₂ / 2.5 h / -30 °C

With [D₃]acetonitrile; water; water-d2; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0040-4020(01)90122-X