N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide

Base Information

Chemical Name:N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide
CAS No.:161220-02-6
Molecular Formula:C₇₃H₇₂N₄O₁₁
Molecular Weight:1181.39
Hs Code.:

Synonyms:N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide

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Chemical Property of N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide

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Technology Process of N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide

There total 3 articles about N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 74272-81-4
2,3-bis(benzyloxy)-N-(3-(4-(2,3-bis(benzyloxy)benzamido)butylamino)propyl)benzamide

: 1027343-22-1
2,3-dibenzyloxybenzoyl-L-serine

: 161220-02-6
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide

Guidance literature:: With dmap; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; 1.) 0 deg C; 2.) rt., 2 d;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 69146-58-3
2,3-bis(benzyloxy)benzoyl chloride

: 161220-02-6
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide

Guidance literature:: Multi-step reaction with 3 steps

2: aq. sodium hydroxide

3: 89 percent / 1.) diphenylphosphoryl azide; 2.) triethylamine, dimethylaminopyridine / dimethylformamide / 1.) 0 deg C; 2.) rt., 2 d

With dmap; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85669-6

Reference yield:

: 1027343-34-5
2,3-dibenzyloxybenzoyl-L-serine methyl ester

: 161220-02-6
N-<3-(2,3-dibenzyloxybenzoylamino)propyl>-N-<4-(2,3-dibenzyl-oxybenzoylamino)butyl>-2,3-dibenzyloxybenzoyl-L-serylamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. sodium hydroxide

2: 89 percent / 1.) diphenylphosphoryl azide; 2.) triethylamine, dimethylaminopyridine / dimethylformamide / 1.) 0 deg C; 2.) rt., 2 d

With dmap; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85669-6