N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide

Base Information

Chemical Name:N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide
CAS No.:1093987-91-7
Molecular Formula:C₂₂H₁₆BrCl₂FN₂O₄
Molecular Weight:542.188
Hs Code.:

Synonyms:N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide

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Chemical Property of N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide

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Technology Process of N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide

There total 9 articles about N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874974-99-9
2-{3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetohydrazide

: 586-38-9
3-Methoxybenzoic acid

: 1093987-91-7
N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 33863-76-2
1-bromo-3-chloro-5-fluorobenzene

: 1093987-91-7
N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide

Guidance literature:: Multi-step reaction with 9 steps

1.1: N,N-dimethyl-formamide / 20 °C

2.1: boron tribromide / dichloromethane / 20 °C

2.2: 20 °C

3.1: sodium t-butanolate / tetrahydrofuran / 0.25 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

4.2: 0 - 20 °C

5.1: trifluoroacetic acid / dichloromethane / 0.75 h / 0 - 60 °C

5.2: 0 °C

6.1: sodium dithionite / tetrahydrofuran; water / 1 h / 20 °C

7.1: tert.-butylnitrite; copper dichloride / acetonitrile / 0.25 h / 50 °C

8.1: hydrazine / ethanol / 8 h / Reflux

9.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C

With tert.-butylnitrite; sodium dithionite; boron tribromide; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; copper dichloride; sodium t-butanolate; hydrazine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 174913-12-3
1-bromo-3-chloro-5-methoxybenzene

: 1093987-91-7
N'-({3-[(3-bromo-5-chlorophenyl)oxy]-4-chloro-2-fluorophenyl}acetyl)-3-(methyloxy)benzohydrazide

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron tribromide / dichloromethane / 20 °C

1.2: 20 °C

2.1: sodium t-butanolate / tetrahydrofuran / 0.25 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 0.75 h / 0 - 60 °C

4.2: 0 °C

5.1: sodium dithionite / tetrahydrofuran; water / 1 h / 20 °C

6.1: tert.-butylnitrite; copper dichloride / acetonitrile / 0.25 h / 50 °C

7.1: hydrazine / ethanol / 8 h / Reflux

8.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C

With tert.-butylnitrite; sodium dithionite; boron tribromide; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; copper dichloride; sodium t-butanolate; hydrazine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;