6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one

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Chemical Name:6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one
CAS No.:1615227-24-1
Molecular Formula:C₂₇H₃₀N₄O₃S
Molecular Weight:490.626
Hs Code.:

Synonyms:6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one

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Chemical Property of 6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one

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Technology Process of 6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one

There total 6 articles about 6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1932-03-2
2-(piperidin-4-yl)ethyl chloride

: 1186078-59-0
6-(4-methoxybenzyl)-3-(3-methyl-4-hydroxyphenyl)thiazolo[3,2-b]-1,2,4-triazin-7-one

: 1615227-24-1
6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one

Guidance literature:: With potassium carbonate; potassium iodide; In acetone; for 24h; Reflux;
DOI:10.1016/j.ejmech.2014.05.020

Reference yield:

: 112517-73-4
6-[(4-methoxyphenyl)methyl]-3,4-dihydro-3-thioxo-1,2,4-triazin-5(2H)-one

: 1615227-24-1
6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / acetic acid / Reflux

2: potassium carbonate / acetone / Reflux

With sodium acetate; potassium carbonate; In acetic acid; acetone;
DOI:10.1111/cbdd.12362

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1615227-24-1
6-(4-methoxybenzyl)-3-{3-methyl-4-[2-(1-piperidinyl)ethoxy]phenyl}-7H-thiazolo[3,2-b]-1,2,4-triazin-7-one

Guidance literature:: Multi-step reaction with 6 steps

1: sodium acetate; acetic anhydride / 7 h / 120 °C

2: water / acetone / 10 h / Reflux

3: hydrogenchloride / water / 10 h / Reflux

4: sodium hydroxide / ethanol / 2 h / Reflux

5: sodium acetate / acetic acid / Reflux

6: potassium carbonate / acetone / Reflux

With hydrogenchloride; water; sodium acetate; acetic anhydride; potassium carbonate; sodium hydroxide; In ethanol; water; acetic acid; acetone;
DOI:10.1111/cbdd.12362