4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane

Base Information

Chemical Name:4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane
CAS No.:1295503-62-6
Molecular Formula:C₂₁H₁₇ClN₂O₃
Molecular Weight:380.831
Hs Code.:

Synonyms:4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane

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Technology Process of 4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane

There total 1 articles about 4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1208262-86-5
C₁₅H₁₂ClNO₂

: 95-85-2
2-hydroxy-5-chloro-aniline

: 1295503-62-6
4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane

Guidance literature:: With triethylamine; In methanol; ethanol; at -5 - 20 ℃;
DOI:10.1134/S0036023610040078

Reference yield: 97.0%

: 1295503-62-6
4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane

: 6046-93-1
copper(II) acetate monohydrate

: [Cu₂(4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane(-2H))2(H₂O)2]*2H₂O

Guidance literature:: With KOH; In ethanol; soln. of equiv. amt. of metal salt in EtOH added to hot soln. of ligand in EtOH; stirred; equiv. amts. of KOH added dropwise to adjust pH value of about 5-6; kept on water bath at 80°C for 1 h; cooled to ambient temp.; solid filtered off; washed (hot H2O, EtOH); dried (P2O5); elem. anal.;
DOI:10.1134/S0036023610040078

Reference yield: 70.0%

: 1295503-62-6
4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: [Co₂(4-(2-hydroxo-5-chlorophenylaminoisonitrosoacetyl)diphenylmethane(-2H))2(H₂O)2]*2H₂O

Guidance literature:: With KOH; In ethanol; soln. of equiv. amt. of metal salt in EtOH added to hot soln. of ligand in EtOH; stirred; equiv. amts. of KOH added dropwise to adjust pH value of about 5-6; kept on water bath at 80°C for 1 h; cooled to ambient temp.; solid filtered off; washed (hot H2O, EtOH); dried (P2O5); elem. anal.;
DOI:10.1134/S0036023610040078