N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide

Base Information

Chemical Name:N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide
CAS No.:849064-61-5
Molecular Formula:C₁₆H₁₃N₃O₅
Molecular Weight:327.296
Hs Code.:

Synonyms:N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide

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Technology Process of N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide

There total 3 articles about N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.5%

: 38253-40-6
4-amino-4-azatricyclo[5.2.1.0^2,6-endo]dec-8-ene-3,5-dione

: 122-04-3
4-nitro-benzoyl chloride

: 849064-61-5
N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide

Guidance literature:: With pyridine;
DOI:10.1007/s11178-005-0305-9

Reference yield: 51.0%

: 636-97-5
N-amino-(4-nitrophenyl)carboxamide

: 129-64-6
3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

: 849064-61-5
N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide

Guidance literature:: With sulfuric acid; In ethanol; Heating;
DOI:10.1023/B:RUJO.0000045895.04509.2d

Reference yield:

: 129-64-6
3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

: 849064-61-5
N-(p-nitrobenzoylamino)bicyclo[2.2.1]hept-2-ene-endo,endo-5,6-dicarboximide

Guidance literature:: Multi-step reaction with 2 steps

1: 92.5 percent / hydrazine hydrate / benzene; H₂O

2: 93.5 percent / pyridine

With pyridine; hydrazine hydrate; In water; benzene;
DOI:10.1007/s11178-005-0305-9