(3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one

Base Information

Chemical Name:(3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one
CAS No.:162889-21-6
Molecular Formula:C₂₅H₃₄O₆Si
Molecular Weight:458.627
Hs Code.:

Synonyms:(3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one

Suppliers and Price of (3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one

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Technology Process of (3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one

There total 6 articles about (3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 102717-31-7
(2S,4S)-5-(t-butyldiphenylsiloxy)-2-hydroxypentan-4-olide

: 162889-21-6
(3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; Ambient temperature;
DOI:10.1016/0040-4039(94)02209-T

Reference yield:

: 87-72-9,608-45-7,608-46-8,608-47-9,2460-44-8,6748-95-4,6763-34-4,7261-26-9,7283-06-9,7283-07-0,7296-55-1,7296-56-2,7296-58-4,7296-59-5,7296-60-8,7296-61-9,7296-62-0,7322-30-7,10257-31-5,10257-32-6,10257-33-7,10257-34-8,10257-35-9,19982-83-3,20242-88-0,28697-53-2,36562-42-2,41546-41-2,89299-64-9,107655-34-5,115794-06-4,115794-07-5,130550-15-1,130606-21-2
D-Xylose

: 162889-21-6
(3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 6 steps

1: Br₂, K₂CO₃ / H₂O / Ambient temperature

2: acetic acid / 50 °C

3: 97 percent / H₂, Et₃N / Pd/C / ethyl acetate / Ambient temperature

4: 90 percent / KOH, H₂O / ethanol / Ambient temperature

5: 95 percent / imidazole / dimethylformamide / Ambient temperature

6: 97 percent / (iPr)2NEt / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; potassium hydroxide; water; hydrogen; bromine; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; dichloromethane; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(94)02209-T

Reference yield:

D-xylono-1,5-lactone: 82796-87-0
D-xylono-1,5-lactone

: 162889-21-6
(3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-(2-methoxy-ethoxymethoxy)-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 50 °C

2: 97 percent / H₂, Et₃N / Pd/C / ethyl acetate / Ambient temperature

3: 90 percent / KOH, H₂O / ethanol / Ambient temperature

4: 95 percent / imidazole / dimethylformamide / Ambient temperature

5: 97 percent / (iPr)2NEt / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; potassium hydroxide; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(94)02209-T