N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

Base Information

Chemical Name:N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine
CAS No.:1381770-35-9
Molecular Formula:C₂₄H₃₀N₈O₂
Molecular Weight:462.555
Hs Code.:

N<sub>2</sub>-mesityl-N<sub>4</sub>-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

Synonyms:N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

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Chemical Property of N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

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Technology Process of N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

There total 4 articles about N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.1%

: 1352804-13-7
N₂-mesityl-N₄-(piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

: 100-14-1
4-nitrobenzyl chloride

: 1381770-35-9
N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2012.04.030

Reference yield:

: 88-05-1
2,4,6-trimethylaniline

: 1381770-35-9
N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / tetrahydrofuran / 3 h / 0 °C

2.1: sodium hydrogencarbonate / tetrahydrofuran; water; acetone / 8 h / 30 °C

3.1: ammonia / tetrahydrofuran; water / 5 h / 100 °C / Autoclave

4.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

4.2: pH 8

5.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

With ammonia; sodium hydrogencarbonate; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2012.04.030

Reference yield:

: 1352804-07-9
6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine

: 1381770-35-9
N₂-mesityl-N₄-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia / tetrahydrofuran; water / 5 h / 100 °C / Autoclave

2.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

2.2: pH 8

3.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

With ammonia; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.04.030