O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate

Base Information

• Chemical Name: O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate
• CAS No.: 107968-41-2
• Molecular Formula: C₁₄H₂₁O₃P
• Molecular Weight: 268.293
• Mol file: 107968-41-2.mol

Synonyms:O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate

Chemical Property of O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate

There total 5 articles about O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl propylphosphonate (18812-51-6) → O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate (107968-41-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) LDA / 1.) THF, hexane, -60 deg C, 10 min, 2.) THF, -70 deg C, 15 min

2: tetrahydrofuran / 2 h / Ambient temperature

With lithium diisopropyl amide; In tetrahydrofuran;

DOI:10.1055/s-1986-31828

Reference yield:

diethyl propylphosphonate (18812-51-6) + benzaldehyde (100-52-7) → O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate (107968-54-7) + O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate (107968-41-2)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1080/00397919108021594

Reference yield:

C10H24LiO3PSi + benzaldehyde (100-52-7) → O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate (107968-54-7) + O,O-diethyl ethyl-1 phenyl-2 ethenyl-1,2 phosphonate (107968-41-2)

Guidance literature:

In tetrahydrofuran; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1055/s-1986-31828

upstream raw materials:

diethyl propylphosphonate

benzaldehyde

Diethyl phosphonate

2-oxo-1-phenylbutylphosphonate de diethyle