N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester

Base Information

Chemical Name:N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester
CAS No.:220079-68-5
Molecular Formula:C₁₆H₂₅N₃O₅S
Molecular Weight:371.458
Hs Code.:

Synonyms:N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester

Suppliers and Price of N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester

There total 3 articles about N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4083-64-1
Tosyl isocyanate

: 220079-64-1
1-(tert-butoxycarbonyl)-1-ethyl-2-methylhydrazine

: 220079-68-5
N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: In dichloromethane;
DOI:10.1055/s-1998-2217

Reference yield:

: 127799-53-5
1-[(1,1-dimethylethoxy)carbonyl]-2-[(phenylmethoxy)carbonyl]-2-methylhydrazine

: 220079-68-5
N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / K₂CO₃, Bu₄NHSO₄, NaOH / benzene / 30 h / Ambient temperature

2: 89 percent / H₂ / 5percent Pd/C / methanol

3: 97 percent / CH₂Cl₂

With sodium hydroxide; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane; benzene;
DOI:10.1055/s-1998-2217

Reference yield:

: 220079-14-1
1-(benzyloxycarbonyl)-2-(tert-butoxycarbonyl)-2-ethyl-1-methylhydrazine

: 220079-68-5
N-Ethyl-N'-methyl-N'-(toluene-4-sulfonylaminocarbonyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / H₂ / 5percent Pd/C / methanol

2: 97 percent / CH₂Cl₂

With hydrogen; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1055/s-1998-2217