(E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol

Base Information

Chemical Name:(E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol
CAS No.:548483-77-8
Molecular Formula:C₂₁H₃₀O₃
Molecular Weight:330.467
Hs Code.:

Synonyms:(E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol

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Chemical Property of (E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol

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Technology Process of (E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol

There total 20 articles about (E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 548483-76-7
(E)-4-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-but-2-enal

: 548483-77-8
(E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol

Guidance literature:: In diethyl ether; at -78 ℃; for 4h;
DOI:10.1021/ol034619s

Reference yield:

: 548483-74-5
(3S,5S)-1-phenyl-7-octene-3,5-diol

: 548483-77-8
(E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / CSA / acetone / 0.33 h / 25 °C

2: 70 percent / imidazolidine-based ruthenium metathesis catalyst / CH₂Cl₂ / 25 °C

3: 84 percent / diethyl ether / 4 h / -78 °C

With imidazolidine-based ruthenium metathesis catalyst; camphor-10-sulfonic acid; In diethyl ether; dichloromethane; acetone;
DOI:10.1021/ol034619s

Reference yield:

: 548483-75-6
(4S,6S)-4-Allyl-2,2-dimethyl-6-phenethyl-[1,3]dioxane

: 548483-77-8
(E)-(R)-7-((4S,6S)-2,2-Dimethyl-6-phenethyl-[1,3]dioxan-4-yl)-hepta-1,5-dien-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / imidazolidine-based ruthenium metathesis catalyst / CH₂Cl₂ / 25 °C

2: 84 percent / diethyl ether / 4 h / -78 °C

With imidazolidine-based ruthenium metathesis catalyst; In diethyl ether; dichloromethane;
DOI:10.1021/ol034619s