1-{4-[N',N''-di(tert-butoxycarbonyl)guanidino]phenyl}-3-(4-aminophenyl)urea

Base Information

• Chemical Name: 1-{4-[N',N''-di(tert-butoxycarbonyl)guanidino]phenyl}-3-(4-aminophenyl)urea
• CAS No.: 1196966-10-5
• Molecular Formula: C₂₄H₃₂N₆O₅
• Molecular Weight: 484.555

Synonyms:1-{4-[N',N''-di(tert-butoxycarbonyl)guanidino]phenyl}-3-(4-aminophenyl)urea

Chemical Property of 1-{4-[N',N''-di(tert-butoxycarbonyl)guanidino]phenyl}-3-(4-aminophenyl)urea

Chemical Property:

Purity/Quality:

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Technology Process of 1-{4-[N',N''-di(tert-butoxycarbonyl)guanidino]phenyl}-3-(4-aminophenyl)urea

There total 1 articles about 1-{4-[N',N''-di(tert-butoxycarbonyl)guanidino]phenyl}-3-(4-aminophenyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

N,N'-bis(4-aminophenyl)urea (4550-72-5) + tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate (145013-05-4) → 1-{4-[N',N''-di(tert-butoxycarbonyl)guanidino]phenyl}-3-(4-aminophenyl)urea (1196966-10-5)

Guidance literature:

With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1021/jm901017t

Reference yield: 65.0%

1-{4-[N',N''-di(tert-butoxycarbonyl)guanidino]phenyl}-3-(4-aminophenyl)urea (1196966-10-5) + 2-thioxo-imidazolidine-1,3-dicarboxylic acid di-tert-butyl ester (173300-83-9) → C37H52N8O9 (1196966-18-3)

Guidance literature:

With triethylamine; mercury dichloride; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jm901017t

upstream raw materials:

N,N'-bis(4-aminophenyl)urea

tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate

Downstream raw materials:

C₃₇H₅₂N₈O₉

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