Technology Process of C26H43N3O8
There total 6 articles about C26H43N3O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water;
at 20 - 50 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -10 - 0 °C
2.1: triethylamine / dichloromethane / 0.5 h / 0 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C
3.2: 12.5 h / -10 - 20 °C
4.1: water; zinc; ammonium chloride / tetrahydrofuran / 8 h / 20 °C
5.1: water / 20 - 50 °C
With
water; potassium carbonate; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; zinc;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium azide; triphenylphosphine / tetrachloromethane; N,N-dimethyl-formamide / 90 °C
1.2: 0.17 h / 20 °C
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / -10 - 0 °C
3.1: triethylamine / dichloromethane / 0.5 h / 0 °C
4.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C
4.2: 12.5 h / -10 - 20 °C
5.1: water; zinc; ammonium chloride / tetrahydrofuran / 8 h / 20 °C
6.1: water / 20 - 50 °C
With
sodium azide; water; potassium carbonate; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; zinc;
In
tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;