Technology Process of (C6H5)2Sn(C6H4(O)CHNNCONH2)
There total 2 articles about (C6H5)2Sn(C6H4(O)CHNNCONH2) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
NaOCH3;
In
methanol; benzene;
byproducts: NaCl; dropwise addn. of ligand in abs. MeOH/C6H6 (3:1) to NaOCH3 soln. (under N2); stirring 1h; addn. of Ph3SnCl in MeOH; stirring 1h; refluxing 3-4h; cooling; centrifugation; concg. clear soln. by distn.; pptn.; filtration; recrystn. (MeOH); drying in vac. (P2O5); elem. anal.;
- Guidance literature:
-
With
sodium methylate;
In
methanol; benzene;
under N2; soln. of ligand in MeOH is added under stirring to soln. of NaOCH3 in MeOH, stirred for 1 h, solvent removed under reduced pressure, residue is suspended in benzene, dropwise addn. of benzene soln. of Sn-compd. under refluxing (4 h); filtn., evapn. (vac.), crystn., washing (petroleum ether), vac.-drying; elem. anal.;
